WHAT IS THE STANDARD Opearating procedure of FT-IR analysis.

Question

Accepted Answer

The standard operating procedure of FT-IR analysis involves sample preparation, instrument calibration, data acquisition, and interpretation.

Sample preparation involves obtaining a representative sample and preparing it for analysis.
Instrument calibration ensures accurate measurements by calibrating the instrument using known reference materials.
Data acquisition involves placing the sample in the FT-IR instrument and collecting the infrared spectrum.
Interpretation of the obtained spectrum involves comparing it with reference spectra or using spectral databases to identify functional groups and compounds.

Accepted Answer

There is two methods
For solid sample we may use Pottassium Bromide Pellet method. For that in 1:10ratio we use sample and KBr. And by using morter pestle and hydrolic press we prepared.desired pellet. And then by using pellet holder insert it to the Ft IR macine. Then we analysed it with softwares...
company Bruker shimadzu...
softs opus,

for liquid semisolid 
we use ATR unit of the macine..there we directly analysis with or without diluents ( mineral oils/ nujol mull ).
The ZnSi or Diamond plate use.for.sample.insert and scan.
then.analysed by software.

WHAT IS THE STANDARD Opearating procedure of FT-IR analysis.

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