1. What were the issues you faced during developing an analytical method? How did you solve it.

Question

Accepted Answer

During the development of an analytical method, I faced issues with instrument calibration and sample preparation.

One issue I encountered was inconsistent instrument calibration, which resulted in inaccurate measurements. To solve this, I thoroughly checked the calibration procedure and recalibrated the instrument as needed.
Another challenge was optimizing the sample preparation process to ensure reliable and reproducible results. I experimented with different extraction techniques and parameters to find the most suitable method.
I also faced difficulties in selecting the appropriate analytical technique for a specific analyte. To overcome this, I conducted extensive literature research and consulted with experts in the field.
In some cases, I encountered interferences from matrix components that affected the accuracy of the analysis. To address this, I employed sample clean-up techniques such as solid-phase extraction or liquid-liquid extraction.
Furthermore, troubleshooting instrument malfunctions and software issues were common hurdles. I collaborated with the instrument manufacturer's technical support team and utilized troubleshooting guides to resolve these problems.

Accepted Answer

In laboratories abiotic factors like temperature, pressure, time are the main issue. So I have changed the experimental period as per the demand of technique.

Accepted Answer

Highlighting of Steps,Choosing an Analytical Method,Optimization of the Method

Accepted Answer

During injecting sample we didn't get accurate reading

1. What were the issues you faced during developing an analytical method? How did you solve it.

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